Batch Distillation

Distillation Columns

Batch Distillation

Switch Column

Scope
  • Distillations for parameter finding/cut temperature determination
  • Preliminary tests for selecting suitable column type
Operating Parameters
  • Glass column – Batch operation
    • Pressure: 1 mbar to atmospheric pressure
    • Temperature: Room temperature to 350 °C (electrical heating)
    • Feed volume: min. 300 mL (500 mL flask), 1 L flask
    • Sample fractionation
    • Packed column, annular gap column or random packing column

Bubble Tray Column

Scope
  • Distillations (ability to determine concentration on each tray)
Operating Parameters
  • Glass column – continuous or batch operation
    • Pressure: Atmospheric pressure
    • Temperature: Room temperature to 350 °C (electrical heating)
    • Feed rate: approximately 500 mL/h
    • Liquid and gas sampling possible on each tray

Crude Oil Distillation Column

ASTM D2892

We offer crude oil distillation according to the standard procedure ASTM D2892.

This distillation includes the following services:
  • Feed volume: 4 L, 6 L and 10 L
  • Dewatering (if water content exceeds 0.3%)
  • Debutanization at -45 °C
  • Distillation in the range of 15 to 370°C
    (vacuum range: 2 mmHg)
  • Collection of fractions according to your specifications
    (max. 20 cuts)
  • Distillation curve (vol % and mass %), quantity measurement and density determination
  • Analysis of cuts according to your specifications
  • Filling, packaging and shipping of cuts
ASG Circular
about Crude Oil Distillation

Crude Oil Distillation Column

ASTM D5236

We offer crude oil distillation according to the standard procedure ASTM D5236.

This distillation includes the following services:
  • Feed volume: 4 L, 6 L and 10 L
  • Vacuum range: 10 mmHg to 0.1 mmHg
  • Distillation in the range of 370 – 560 °C
  • Collection of fractions according to your specifications
    (max. 20 cuts)
  • Quantity measurement and density determination
  • Analysis of cuts according to your specifications
  • Filling, packaging and shipping of cuts
ASG Circular
about Crude Oil Distillation

Column PD150S

Scope
  • Distillation of highly viscous liquids and bituminous residues
Operating Parameters
  • Stainless steel column with batch operation
    • Pressure: Atmospheric pressure and vacuum
    • Bottom volume: 20 L
    • Temperature: Room temperature to 400 °C AET (electrical heating)
    • Bottom drain
    • 2 theoretical separation stages
Contact
Alina Greve
Alina Greve
Head of Miniplant LAB & Synthesis Department
Contact
Christian Schwarz
Christian Schwarz
Head of Miniplant Laboratory & Testing Fuel Department

Need additional analyses?

Our laboratory has been accredited since 1998 for the analysis of numerous fossil and biogenic fuels.